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Поволжская археология

Local and Integral Techniques in Metal Compositional Analysis of Archaeological Objects with Surface Corrosion Layers and Small Sample Quantities

Loboda A.Yu., Tereshchenko E.Yu. (Moscow, Russian Federation), Antipenko A.V. (Simferopol, Russian Federation), Retivov V.M., Presniakov M.Yu., Kolobylina N.N., Kondratiev O.A., Shishlina N.I., Yatsishina E.B., Kashkarov P.K. (Moscow, Russian Federation)


page 203–221

UDC 902/904; 7.021; 548; 620.187; 543.51; 543.05

DOI: https://doi.org/10.24852/2018.4.26.203.221


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The paper presents the difference of three varied methods which have been used to analyze archaeological metals: X-ray fluorescence analysis – XRF (X-ray spectrometer), energy dispersive X-Ray microanalysis – EDAX (electron microscopy), and inductively coupled plasma mass spectrometry (MS-ICP). Illustrative examples of different measurements are two fragments of sickles from the hoard near the village of Sosnovaya Maza and three plates of horse harness from the treasure from the territory of the Republic of Crimea. The analysis of the results reveals the importance of formulation an individual methodology for analysis and the process of sample preparation for each measured object.

Keywords

archaeologyhoard near the village of Sosnovaya Mazadetails of horse equipmentX-ray fluorescencescanning electron microscopymass spectrometry with inductive plasma

About the author(s)

Loboda Anastasiya Yu. National Research Center «Kurchatov Institute». Akademik Kurchatov Sq., 1, Moscow, 123182, Russian Federation; lobodaau@mail.ru

Tereshhenko Elena Yu. Candidate of Physical and Mathematical Sciences, National Research Center «Kurchatov Institute». Akademik Kurchatov Sq., 1, Moscow, 123182, Russian Federation; Federal Research Center "Crystallography and Photonics". Leninsky Prospect, 59, Moscow, 119333, Russian Federation; elenatereschenko@yandex.ru

Antipenko Anna V. V.I. Vernadsky Crimean Federal University, Vernadskogo Pr., 4, Simferopol, 295007, Crimea, Russian Federation; an.antipenko@yandex.ru

Retivov Vasiliy M. Candidate of Chemical Sciences, National Research Center «Kurchatov Institute». Akademik Kurchatov Sq., 1, Moscow, 123182, Russian Federation; vasilii_retivov@mail.ru

Presnyakov Mikhail Yu. National Research Center «Kurchatov Institute». Akademik Kurchatov Sq., 1, Moscow, 123182, Russian Federation; mpresniakov@gmail.com

Kolobylina Natal'ya N. National Research Center «Kurchatov Institute». Akademik Kurchatov Sq., 1, Moscow, 123182, Russian Federation; kolobylina@gmail.com

Kondrat'ev Oleg A. National Research Center «Kurchatov Institute». Akademik Kurchatov Sq., 1, Moscow, 123182, Russian Federation; FNITs «Kristallografiya i fotonika» RAN (g. Moskva, Rossiya); edelier@mail.ru

Shishlina Natal'ya I. Doctor of Historical Sciences, State Historical Museum. Red Sq., 1, Moscow, 109012, Russian Federation; nshishlina@mail.ru

Yatsishina Ekaterina B. Candidate of Philosophy. National Research Center «Kurchatov Institute». Akademik Kurchatov Sq., 1, Moscow, 123182, Russian Federation; yatsishina_eb@nrcki.ru

Kashkarov Pavel K. Doctor of Physical and Mathematical Sciences, National Research Center «Kurchatov Institute». Akademik Kurchatov Sq., 1, Moscow, 123182, Russian Federation; kashkarov_pk@nrcki.ru